Reaction of phenylacetylene with a di-µ-hydroxo-di-copper(II) complex of a macrocyclic ligand affords diphenyldiacetylene together with a tetranuclear copper(I) complex containing a Cu4-phenylacetylide core in which the terminal carbon atom is five-co-ordinate.
M. G. B. Drew, F. S. Esho and S. M. Nelson, J. Chem. Soc., Chem. Commun., 1982, 1347 DOI: 10.1039/C39820001347
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