SCHEDULED MAINTENANCE
Treatment of propargyl chloride with methyl-lithium and an excess of alkyl chloroformate leads to chlorotetrolic esters in an average yield of 65%, in contrast with the previously reported three-step, low-yield synthesis of these biochemical reagents.
M. Olomucki, J. le Gall and I. Barrand, J. Chem. Soc., Chem. Commun., 1982, 1290 DOI: 10.1039/C39820001290
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