Iodine-127 Mössbauer spectroscopic data are used to show that at low temperature, the [I2+] cation in flourosulphuric acid dimerises to the [I42+] cation; the frozen solution data are compared with those for authentic [I42+] salts.
T. Brichall and R. D. Myers, J. Chem. Soc., Chem. Commun., 1982, 1174 DOI: 10.1039/C39820001174
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