Treatment of an Sb-Sn mixed oxide, calcined at 750 °C, with dil. HCl greatly improves the mild oxidation of propene to acrolein; it has been shown that large α-Sb2O4 particles, formed during the high-temperature calcination, do not favour this oxidation.
J. Volta, G. Coudurier, I. Mutin and J. C. Védrine, J. Chem. Soc., Chem. Commun., 1982, 1044 DOI: 10.1039/C39820001044
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