Thiobenzaldehyde and thioacetaldehyde have been generated by thermolysis of alkyl thiosulphinates under preparatively useful conditions and trapped with aromatic and aliphatic 1,3-dienes, the adducts with anthracene being convenient and high yielding sources of such thioaldehydes; thiobenzaldehyde has been shown to undergo the ‘ene’ reaction.
J. E. Baldwin and R. C. G. Lopez, J. Chem. Soc., Chem. Commun., 1982, 1029 DOI: 10.1039/C39820001029
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