Electrocatalytic addition of perfluoroalkyl iodides to 3-hydroxy-3-alkylbut -1-ynes, followed by dehydroiodination and thermal cleavage in basic medium, leads to an easy and efficient preparation of (perfluoroalkyl)alkynes.
P. Calas, P. Moreau and A. Commeyras, J. Chem. Soc., Chem. Commun., 1982, 433 DOI: 10.1039/C39820000433
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