The trianion [Re7C(CO)21]3–, isolated from the pyrolysis of [ReH2(CO)4][NEt4] in n-tetradecane, has been characterized by an X-ray crystal structural analysis of the [PPh4]+ salt, and shown to contain a monocapped octahedral arrangement of rhenium atoms with an encapsulated carbon atom.
G. Ciani, G. D. Alfonso, M. Freni, P. Romiti and A. Sironi, J. Chem. Soc., Chem. Commun., 1982, 339 DOI: 10.1039/C39820000339
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