Single-crystal i.r.-reflectance spectroscopy in polarized light has been used to arrive at a definitive assignment of solid Mo(CO)6 in the ν(CO) region.
D. M. Adams, B. M. Peake and I. D. Taylor, J. Chem. Soc., Chem. Commun., 1982, 240 DOI: 10.1039/C39820000240
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