The reversible dioxygenation of Mn(PR3)X2(R = n-butyl, n-pentyl, X = Cl, Br, I) has been studied in solution by e.s.r. spectroscopy; the dioxygenated species, ‘Mn(PR3)(O2)X2,’ have the highly unusual spin state S= 5/2.
C. A. McAuliffe, M. G. Little and J. B. Raynor, J. Chem. Soc., Chem. Commun., 1982, 68 DOI: 10.1039/C39820000068
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