SCHEDULED MAINTENANCE
Thermal decomposition of a variety of 1,3-benzodithiol-2-yl azides (2), easily obtainable from 1,3-benzodithiolylium salts and sodium azide, gives 1,4,2-benzodithiazines (3) in good yields, thus providing a general synthetic route to these compounds.
J. Nakayama, M. Ochiai, K. Kawada and M. Hoshino, J. Chem. Soc., Perkin Trans. 1, 1981, 618 DOI: 10.1039/P19810000618
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