α-Glycols are smoothly cleaved by a catalytic amount of triphenylbismuth in the presence of potassium carbonate and a little water, using N-bromosuccinimide (or another N-bromo-reagent) for the oxidation of BiIII to BiV.
D. H. R. Barton, W. B. Motherwell and A. Stobie, J. Chem. Soc., Chem. Commun., 1981, 1232 DOI: 10.1039/C39810001232
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