The solvolysis of 3β-p-tolylsulphonyloxyandrost-5-enes in acetic acid containing sodium acetate, is retarded by the presence of a 4β-acetoxy- or hydroxy-group. The products of solvolysis include the A-nor-3-formyl-steroids except in the presence of a 7-ketone.
J. R. Hanson and H. J. Wadsworth, J. Chem. Soc., Perkin Trans. 1, 1980, 933 DOI: 10.1039/P19800000933
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