Carbohydrate derivatives containing a primary nitro-group react with hypochlorite to give αα-dichloronitrocompounds which afford branched-chain cyano-sugars on treatment with triphenylphosphine. The preparation of 3,3-C-bis(nitromethyl) doubly-branched carbohydrate derivatives is also described.
R. H. Hall, A. Jordaan and M. Malherbe, J. Chem. Soc., Perkin Trans. 1, 1980, 126 DOI: 10.1039/P19800000126
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