Reaction of pentakis(t-butyl isocyanide)iron with the hydrido-metal carbonyls [MnH(CO)5] and [OsH2(CO)4] affords the salts [FeH(CNBut)5][Mn(CO)5] and [FeH(CNBut)5][OsH(CO)4], respectively. Protonation of [Fe(CNBut)5] with anhydrous HBF4·2Et2O yields [FeH(CNBut)5][BF4].
J. Bassett, L. J. Farrugia and F. G. A. Stone, J. Chem. Soc., Dalton Trans., 1980, 1789 DOI: 10.1039/DT9800001789
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