The reaction of a mixture of bicyclic ozonides (trioxolans), carbonyl compounds, and hydrogen peroxide in the presence of catalytic amounts of chlorosulphonic acid gives the corresponding 2,3,5,6,11-pentaoxabicyclo[5.3.1]undecanes in 3–35% yield.
M. Miura, A. Ikegami, M. Nojima and S. Kusabayashi, J. Chem. Soc., Chem. Commun., 1980, 1279 DOI: 10.1039/C39800001279
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