Monochloroborane–dimethyl sulphide, BH2Cl.SMe2, is formed in essentially quantitative yield upon reflux of an equimolar mixture of borane–dimethyl sulphide, BH3.SMe2, and tetrachloromethane; it can be used directly for production of dialkylchloroboranes by the hydroboration of alkenes.
W. E. Paget and K. Smith, J. Chem. Soc., Chem. Commun., 1980, 1169 DOI: 10.1039/C39800001169
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