2,6-Dimethyl-18-crown-6 has been prepared in 11% yield by reaction of diallyl ether and tetraethylene glycol with mercury(II) acetate in the presence of perchloric acid and potassium perchlorate, followed by reductive demercuration with alkaline sodium borohydride.
A. J. Bloodworth, D. J. Lapham and R. A. Savva, J. Chem. Soc., Chem. Commun., 1980, 925 DOI: 10.1039/C39800000925
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