Sulphanilamide, a potent inhibitor of the enzyme carbonic anhydrase, showed a photo-CIDNP 1H n.m.r. spectrum; the resultant polarisation was maintained when the ligand was bound to the enzyme and a new resonance, arising from the slowly exchanging bound species, was observed.
R. Kaptein and P. Wyeth, J. Chem. Soc., Chem. Commun., 1980, 538 DOI: 10.1039/C39800000538
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