The interaction of dimolybdenum tetra-acetate, Mo2(O2CMe)4, with sodium amalgam in tetrahydrofuran in the presence of an excess of trimethylphosphine under hydrogen (3 atm) yields the dimeric phosphine hydride (Me3P)3HMo(µ-H)2MoH(PMe3)3, whose structure has been determined by X-ray diffraction methods.
R. A. Jones, K. W. Chiu, G. Wilkinson, A. M. R. Galas and M. B. Hursthouse, J. Chem. Soc., Chem. Commun., 1980, 408 DOI: 10.1039/C39800000408
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