X-Ray crystallography and 195Pt and 31P n.m.r. spectroscopy show that an intensely luminescent product from K2PtCl4–H3PO3 reactions is a dimer with close Pt atoms (2·925 Å) bridged by four P–O–P linkages from diphosphorous acid ligands; its reactions and uses are discussed.
M. A. F. D. R. Pinto, P. J. Sadler, S. Neidle, M. R. Sanderson, A. Subbiah and R. Kuroda, J. Chem. Soc., Chem. Commun., 1980, 13 DOI: 10.1039/C39800000013
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