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The crystal structure of exo-7-hydroxybicyclo[3.3.1]nonan-3-one (III) and exo-7-methoxybicyclo[3.3.1]nonan-3-one (IV) have been determined. The structure of (III) shows distortions which may be caused either by partial 3,7-hydride transfer or by a disordered arrangement of undistorted dimers in the crystal. The structure of (IV) shows no unexpected distortions.
J. Murray-Rust, P. Murray-Rust, William. C. Parker, R. L. Tranter and C. I. F. Watt, J. Chem. Soc., Perkin Trans. 2, 1979, 1496 DOI: 10.1039/P29790001496
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