The molecular structure and interatomic dimensions of [Mo2(O2CCF3)4] in the gas phase at 150 °C have been determined by electron-diffraction measurements and shown to be similar to those obtained by X-ray diffraction methods; dimensions obtained include Mo–Mo 2.105(9), Mo–O 2.102(6)Å, and Mo–Mo–O 91.9(3)°.
C. D. Garner, I. H. Hillier, I. B. Walton and B. Beagley, J. Chem. Soc., Dalton Trans., 1979, 1279 DOI: 10.1039/DT9790001279
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