Reaction of [(η-C5H5)2TiCl2] with (Bun4N)2[Mo2O7] and water in CH2Cl2 yields (Bun4N)3[(η-C5H5)Ti(Mo5O18)], shown to contain the [(η-C5H5)Ti(Mo5O18)]3– anion which is related to the octahedral Mo6O192– anion by replacement of an [MoVIO]4+ sub-unit by [TiIV(η-C5H5)]3+.
W. G. Klemperer and W. Shum, J. Chem. Soc., Chem. Commun., 1979, 60 DOI: 10.1039/C39790000060
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