The X-ray diffractometric methods used by previous workers to analyse positive plate material from lead-acid batteries for α-, β- and amorphous lead dioxides are critically appraised. In addition two alternative approaches, not previously applied to this problem, are assessed. An internal standard method is considered to be the best.
P. R. Skidmore and R. R. Schwarz, Analyst, 1979, 104, 952 DOI: 10.1039/AN9790400952
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