The cluster [H3CoOs3(CO)12] was prepared from the reaction of [H2Os3(CO)10] with [Co4(CO)12] in heptane under reflux; a single crystal X-ray analysis has revealed a tetrahedral arrangement of the four metal atoms with twelve terminally bound CO ligands.
S. Bhaduri, B. F. G. Johnson, J. Lewis, P. R. Raithby and D. J. Watson, J. Chem. Soc., Chem. Commun., 1978, 343 DOI: 10.1039/C39780000343
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