Low-temperature ozonation of aliphatic and aromatic acetals leads to oxygen rich intermediates, the acetal hydrotrioxides (1)–(3), the n.m.r. spectra of which show two OOOH absorptions at ca.δ 13; decomposition of these compounds which affords among other products, singlet oxygen, involves non-radical and radical processes.
F. Kovač and B. Plesničar, J. Chem. Soc., Chem. Commun., 1978, 122 DOI: 10.1039/C39780000122
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