Crystals of (CH3CNO)8 are monoclinic, space group C2/c, with Z= 8 in a unit cell of dimensions a= 23.915(7), b=17.467(6), c= 11.169(4)Å, β= 100.71(6)°. Diffractometer data yielded 2169 observed reflections. The structure was solved by direct methods and refined by a least-squares procedure to R 0.071. The molecule is a cyclic octamer of acetonitrile oxide with anti-CH3 configuration at all double bonds.
S. Menchetti and C. Sabelli, J. Chem. Soc., Perkin Trans. 2, 1977, 334 DOI: 10.1039/P29770000334
To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.
If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.
If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.
Read more about how to correctly acknowledge RSC content.
Please wait while we load your content...