Alkali-metal hexafluoromolybdates(IV), M2[MoF6](M = Li, Na, Rb, or Cs), have been prepared by interaction of equivalent amounts of MoF6 and Ml in sulphur dioxide solution. The potassium salt has been obtained impure, mixed with hexafluoromolybdate(III). Unit-cell dimensions and magnetic susceptibilities of all the compounds have been measured, and i.r. and visible spectra in the case of caesium.
A. J. Edwards and B. R. Steventon, J. Chem. Soc., Dalton Trans., 1977, 1860 DOI: 10.1039/DT9770001860
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