Variable-temperature 13C(carbonyl) and 1H n.m.r. spectra of the title complex [Os3(C6H8)(CO)10] have been recorded. Four independent dynamic processes involving both organic-ligand and carbonyl-site exchange have been shown to occur and the limiting 13CO n.m.r. spectrum leads to a determination of the molecular geometry of the complex.
E. G. Bryan, B. F. G. Johnson and J. Lewis, J. Chem. Soc., Dalton Trans., 1977, 144 DOI: 10.1039/DT9770000144
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