Deuterium labelling experiments show that addition of MeO· to (MeO)2S to produce (MeO)3S· is stereoselective such that the incoming radical takes up an apical site in the adduct.
J. W. Cooper and B. P. Roberts, J. Chem. Soc., Chem. Commun., 1977, 228 DOI: 10.1039/C39770000228
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