Phosphinothioic methanesulphonic anhydrides (1) react with aluminium chloride or bromide to form complexes which after decomposition with water or methanol give halides (2) in high yield, with retention of configuration at phosphorus in the case of aluminium chloride.
J. Michalski and Z. Skrzypczyński, J. Chem. Soc., Chem. Commun., 1977, 66 DOI: 10.1039/C39770000066
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