3,5-Dimethyl-4-vinylisoxazole (3) has been prepared from pentane-2,4-dione by way of 1-(3,5-dimethylisoxazol-4-yl)ethanol (2) by two different methods, one of which gives an overall yield greater than 75%. Compound (3), in the presence of radical initiators, is transformed into polymers with pendant isoxazole rings.
V. Bertini, A. De Munno and M. Pocci, J. Chem. Soc., Perkin Trans. 1, 1976, 570 DOI: 10.1039/P19760000570
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