Diethyl azodicarboxylate is a convenient condensing agent in the synthesis of spirophosphoranes from cyclic PIII compounds and 1,2- or 1,3-glycols. The variable-temperature 1H n.m.r. spectra of some of the new spirophophoranes are discribed.
S. A. Bone and S. Trippett, J. Chem. Soc., Perkin Trans. 1, 1976, 156 DOI: 10.1039/P19760000156
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