Direct photolysis of α-diazobenzylphosphonates in alcohols at 300 K mainly gives the O–H insertion product, whereas in alcoholic matrices at 77 K it results in the C–H insertion product in high yield at the expense of the O–H insertion product.
H. Tomioka, T. Inagaki and Y. Izawa, J. Chem. Soc., Chem. Commun., 1976, 1023 DOI: 10.1039/C39760001023
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