Electrolysis of a mixture of phenylacetylene (1) and alkyl halides in hexamethylphosphoramide containing tetra-n-butylammonium iodide as supporting electrolyte produces the corresponding alkylphenylacetylenes in good yields.
M. Tokuda, T. Taguchi, O. Nishio and M. Itoh, J. Chem. Soc., Chem. Commun., 1976, 606 DOI: 10.1039/C39760000606
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