Issue 12, 1976
From the journal:

Journal of the Chemical Society, Chemical Communications

A distorted trigonal-bipyramidal phosphorane with a diequatorial four-membered ring; X-ray crystal structure of 4-p-bromophenyl-2′,2′,3′,4′,4′-pentamethyl-3,3,6,6-tetrakistrifluoromethyl-2,7-dioxa-1-phospha(V)bicyclo[3,2,0]hept-4-ene-1-spiro-1′-phosph(V)etan

Hassan A. E. Aly,   John H. Barlow,   David R. Russell,   David J. H. Smith,   Mary Swindles  and  Stuart Trippett  

Abstract

hexafluoroacetone and 1-phenylethynylphosphetan gave a 2 : 1 adduct shown by X-ray structure analysis to be a five-co-ordinate phosphorane having distorted trigonal bipyramidal geometry with a diequatorial phosphetan ring.

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Article information

DOI
https://doi.org/10.1039/C39760000449
Article type
Paper

J. Chem. Soc., Chem. Commun., 1976, 449-450

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A distorted trigonal-bipyramidal phosphorane with a diequatorial four-membered ring; X-ray crystal structure of 4-p-bromophenyl-2′,2′,3′,4′,4′-pentamethyl-3,3,6,6-tetrakistrifluoromethyl-2,7-dioxa-1-phospha(V)bicyclo[3,2,0]hept-4-ene-1-spiro-1′-phosph(V)etan

H. A. E. Aly, J. H. Barlow, D. R. Russell, D. J. H. Smith, M. Swindles and S. Trippett, J. Chem. Soc., Chem. Commun., 1976, 449 DOI: 10.1039/C39760000449

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