Oxidative deamination of unbranched primary amines by the combination of alkyl nitrites and anhydrous copper(II) halides in acetonitrile produces geminal dihalides selectively and in synthetically useful yields.
M. P. Doyle and B. Siegfried, J. Chem. Soc., Chem. Commun., 1976, 433 DOI: 10.1039/C39760000433
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