2,3-Germacrenediol, lubimin, and hydroxylubimin, the major stress metabolites of Datura stramonium, incorporate sodium [1,2-13C]acetate in patterns, as shown by 13C n.m.r. spectroscopy, which establish their structures and mevalonate origins; the X-ray structure of hydroxylubimin completely defines its stereochemistry.
G. I. Birnbaum, C. P. Huber, M. L. Post, J. B. Stothers, J. R. Robinson, A. Stoessl and E. W. B. Ward, J. Chem. Soc., Chem. Commun., 1976, 330 DOI: 10.1039/C39760000330
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