Crystals of the title compound are orthorhombic, space group P212121, a= 7·606(1), b= 9·540(1),c= 21.371(1)Å, Z= 4. The structure was solved from diffractometer data by Patterson and heavy-atom methods and refined by full-matrix least-squares to R 0·050 for 1687 independent reflexions. The results confirm the chirality (I) earlier deduced from chemical work and a positive Cotton effect.
M. U. Haque and D. Rogers, J. Chem. Soc., Perkin Trans. 2, 1975, 93 DOI: 10.1039/P29750000093
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