Adamantane chemistry. Part II. X-Ray structure analysis of 5-chloromethyl-4-oxahomoadamantan-5-ol
Abstract
The crystal structure of the title compound was determined by X-ray diffraction from diffractometer data by direct methods. Crystals are monoclinic, space group P21/c, with Z= 4 in a unit cell of dimensions: a= 6·464 ± 0·003, b= 12·927 ± 0·005, c= 12·537 ± 0·004 Å, β= 91·56°β 0·03° the structure was refined by block-diagonal least-squares to R 0·039 for 1435 independent reflections.