1α-Hydroxycorticosterone (5), previously isolated from the skate (genus Raja), has been prepared from corticosterone 21-acetate via its 1,2,6,7-tetradehydro- and 1α,2α-epoxy-6,7-didehydro-derivatives. The configuration at C-1 has been established by polarimetry.
D. E. Kime, J. Chem. Soc., Perkin Trans. 1, 1975, 2371 DOI: 10.1039/P19750002371
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