The formation of 5-chloro-5α-cholestane from cholest-5-ene and hydrogen chloride in ether–ethanol at 25 °C appears to be accompanied by production of an unidentified chloro-5ξ-cholestane; 5-chloro-5β-cholestane could not be isolated.
C. W. Shoppee and R. D. Lundberg, J. Chem. Soc., Perkin Trans. 1, 1975, 2208 DOI: 10.1039/P19750002208
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