Compounds of the type [Fe(NH3)6]X2(X = NO3 or SCN; X2= SO4) have been investigated between 4·2 and 340 K using the 57Fe Mössbauer effect. The experiments suggest two-phase transitions occurring in the nitrate and possibly the thiocyanate which are determined by hindrance to the motion of the NH3, NO3, and SCN groups.
L. Asch, G. K. Shenoy, J. M. Friedt and J. P. Adloff, J. Chem. Soc., Dalton Trans., 1975, 1235 DOI: 10.1039/DT9750001235
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