The preparation of Be(B3H8)2 from TlB3H8 and BeCl2 is reported; a study of its 270 MHz 1H and 87·6 MHz 11B F.T. n.m.r. spectra over a range of temperatures using spin decoupling and line narrowing techniques has resulted in the identification of its low temperature static configuration and intermediate and high temperature fluxional forms.
D. F. Gaines and J. H. Morris, J. Chem. Soc., Chem. Commun., 1975, 626 DOI: 10.1039/C39750000626
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