Diethylene orthocarbonate (3) converts ketones and aldehydes into their corresponding acetals in good yield at room temperature; it is particularly suitable for ortho-hydroxyaromatic aldehydes.
D. H. R. Barton, C. C. Dawes and P. D. Magnus, J. Chem. Soc., Chem. Commun., 1975, 432 DOI: 10.1039/C39750000432
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