Consecutive treatment of [Mn(CO)5]– with methyl isothiocyanate and methyl iodide yields [[graphic omitted]Me}]2; the molecular structure has been determined by X-ray diffraction, and shown to contain a previously unreported bridging chelate ligand.
S. R. Finnimore, R. Goddard, S. D. Killops, S. A. R. Knox and P. Woodward, J. Chem. Soc., Chem. Commun., 1975, 391 DOI: 10.1039/C39750000391
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