SCHEDULED MAINTENANCE
Intramolecular photocycloaddition takes place when a solution of mannitol hexacinnamate is irradiated (λ > 290 nm) and, after ester exchange with excess of methanol and chromatographic separation, methyl cinnamate, dimethyl β-truxinate, (±)-dimethyl neo-truxi-nate, and (+)-dimethyl δ-truxinate are isolated; the optical yield of the latter is as high as 46%
B. S. Green, Y. Rabinsohn and M. Rejtő, J. Chem. Soc., Chem. Commun., 1975, 313 DOI: 10.1039/C39750000313
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