The variable temperature 1H n.m.r. spectra of neopentyl bromide and iodide from –150 to –170 °C show changes in the respective t-butyl resonances consistent with slowing t-butyl rotation on the n.m.r. time scale.
C. H. Bushweller, S. Hoogasian, W. G. Anderson and L. J. Letendre, J. Chem. Soc., Chem. Commun., 1975, 152 DOI: 10.1039/C39750000152
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