Back-titration procedures involving the use of oxidants such as chloramine T, potassium iodate and iodine are described for the accurate assay of sulphurated sodium borohydride. Quantitative reactions are completed within 1 h at room temperature for the concentrations and proportions described. The methods are simple, reproducible and accurate within the limits described.
V. M. S. Ramanujam and N. M. Trieff, Analyst, 1975, 100, 655 DOI: 10.1039/AN9750000655
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