A macrobicyclic polyether (4) has been synthesised from pentaerythritol in four steps and is a suitable precursor to related compounds where the nature of the functional groups attached to the bridgehead carbon atoms can be varied.
A. C. Coxon and J. F. Stoddart, J. Chem. Soc., Chem. Commun., 1974, 537a DOI: 10.1039/C3974000537A
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